By Mario L. Occelli and Harry E. Robson (Eds.)
content material: Molecular sieve technological know-how and know-how : a historic point of view / Robert M. Milton --
Zeolites : their nucleation and progress / R.M. Barrer --
Precursors in zeolite synthesis : a serious evaluation / J.J. Keijsper and M.F.M. submit --
constitution and homes of aluminosilicate strategies and gels / Gillian Harvey and Lesley S. Dent Glasser --
functions of NMR spectroscopy to the research of zeolite synthesis / Alexis T. Bell --
saw and calculated silicate and aluminosilicate oligomer concentrations in alkaline aqueous ideas / P. Caullet and J.L. Guth --
impact of D₂O and alcohols at the crystallization of zeolites / Prabir ok. Dutta, Micky Puri, and Christopher Bowers --
impression of autocatalytic nucleation on zeolite crystallization tactics / B. Subotić --
function of gel getting older in zeolite crystallization / A. Katović, B. Subotić, I. Šmit, Lj. A. Despotović, and M. Ćurić --
Silicate species with cagelike constitution in recommendations and quick solidification with natural quaternary ammonium ions / Isao Hasegawa and Sumio Sakka --
position of the tetramethylammonium cation within the synthesis of zeolites ZK-4, Y, and HS / P.D. Hopkins --
Stabilizing position of linear polyamines as pore fillers in the course of the crystallization of zeolite NU-10 / Concettina Pellegrino, Rosario Aiello, and Zelimir Gabelica --
Zeolite synthesis within the presence of fluoride ions : a comparability with traditional synthesis tools / J.L. Guth, H. Kessler, J.M. Higel, J.M. Lamblin, J. Patarin, A. Seive, J.M. Chezeau, and R. Wey --
Cancrinite crystallization from alkaline aluminosilicate structures containing huge and small cations / C. Colella and M. de' Gennaro --
Nonaqueous synthesis of silica sodalite / D.M. Bibby, N.I. Baxter, D. Grant-Taylor, and L.M. Parker --
Contribution of propylammonium species to the stabilization of the MFI-Type constitution / J. Patarin, H. Kessler, M. Soulard, and J.L. Guth --
impact of gravity on silicalite crystallization / David T. Hayhurst, Peter J. Melling, Wha Jung Kim, and William Bibbey --
Crystallization of pentasil zeolite within the absence of natural templates / Feng-Yuen Dai, Minoru Suzuki, Hiroshi Takahashi, and Yasukazu Saito --
Crystal progress rules and morphology of zeolite unmarried crystals of the MFI style / J.C. Jansen, C.W.R. Engelen, and H. van Bekkum --
Synthesis of pentasil zeolites with and with no natural templates / W. Schwieger, K.-H. Bergk, D. Freude, and H. Pfeifer --
Synthesis of VPI-5 / Mark E. Davis, Consuelo Montes, and Juan M. Garces --
Synthesis of microporous silicoaluminophosphates in hexanol-water biphasic structures / Johan A. Martens, Bart Verlinden, Machteld Mertens, Piet J. Grobet, and Peter A. Jacobs --
Synthesis and characterization of steel aluminophosphate molecular sieves / Stephen T. Wilson and Edith M. Flanigen --
major parameters within the synthesis of huge alkaline-free MFI-type zeolites and AFI-type aluminophosphates / U. Müller, A. Brenner, A. Reich, and K.K. Unger --
Disordered pentasil-type borosilicates : synthesis and characterization / Giovanni Perego, Giuseppe Bellussi, Angela Carati, Roberto Millini, and Vittorio Fattore --
Isomorphous substitution of boron in mordenite and zeolite Y / Thomas R. Gaffney, Ronald Pierantozzi, and Mark R. Seger --
Hydrothermal isomorphous substitution of boron in zeolite ZSM-5/silicalite / Bogdan Sulikowski and Jacek Klinowski --
Isomorphous substitution of iron within the faujasite lattice / P. Ratnasamy, A.N. Kotasthane, V.P. Shiralkar, A. Thangaraj, and S. Ganapathy --
Zeolite chemistry : substitution of iron or titanium for aluminum in zeolites through response with the respective ammonium fluoride salts / Gary W. Skeels and Edith M. Flanigen --
High-silica faujasite by way of direct synthesis / Harry Robson --
Secondary synthesis of faujasitic catalysts / Halimaton Hamdan and Jacek Klinowski --
Quadrupole nutation NMR stories of moment new release faujasitic catalysts / Halimaton Hamdan and Jacek Klinowski --
Mechanism of swift zeolite crystallizations and its functions to catalyst synthesis / Tomoyuki Inui --
Kinetics and mechanism of crystal development of zeolite Omega / F. Fajula, S. Nicolas, F. Di Renzo, C. Gueguen, and F. Figuéras --
Synthesis of the hot large-pore zeolite ECR-1 / D.E.W. Vaughan and K.G. Strohmaier --
Directing parameters within the synthesis of zeolites ZSM-20 and Beta / Zelimir Gabelica, Nicole Dewaele, Lutgarde Maistriau, Janos B. Nagy, and Eric G. Derouane --
Synthesis and characterization of zeolite ZSM-20 / D.E.W. Vaughan, M.M.J. Treacy, J.M. Newsam, K.G. Strohmaier, and W.J. Mortier --
stories at the kinetics of ZSM-23 crystallization / S. Ernst, R. Kumar, and J. Weitkamp --
High-resolution electron microscopic experiences of zeolite ZSM-48 / Angus I. Kirkland, G. Robert Millward, Stuart W. Carr, Peter P. Edwards, and Jacek Klinowski --
aggressive function of natural and inorganic cations in directing one-dimensional zeolitic constructions : ZSM-48 and EU-1 / Girolamo Giordano, Janos B. Nagy, Eric G. Derouane, Nicole Dewaele, and Zelimir Gabelica --
section identity of hydrothermal crystallization items from M₂O-SiO₂-SnO₂-H₂O gels or suggestions / Edward W. Corcoran, Jr., J.M. Newsam, H.E. King, Jr., and D.E.W. Vaughan --
Computational reviews of zeolite framework balance / R.A. van Santen, G. Ooms, C.J.J. den Ouden, B.W. van Beest, and M.F.M. Post.
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Additional resources for Zeolite Synthesis
Example text
Since the occurrence and d i s t r i b u t i o n of defect s i t e s may give a clue about the operating synthesis mechanism ( c f . the introductory comments and Figure 1) they have been studied i n closer d e t a i l . F i r s t , the dependence of the number of defects on the A l con tent was determined by Si-NMR spectroscopy applied to various ZSM-5 samples having d i f f e r e n t S i / A l r a t i o s . In Table IV these r a t i o s are indicated, together with the percentage i n t e n s i t y of the Si-NMR resonance centered around -103 ppm.
E . 5, which i s a normal value f o r S i - r i c h z e o l i t e synthesis mixtures) the larger part of the s i l i c a t e species present i n solution consists of uncharacter i z e d , polymeric s i l i c a t e s . The values obtained i n the absence of DMSO (lower part of Table III and Figures 2a and 2b are i n good agreement with l i t e r a t u r e findings (14). ch003 1 2 Basic S i l i c a t e Solutions: Dynamics. Exchange reactions between s i l i c a t e s as well as z e o l i t e formation involve condensation and hydrolysis reactions between dissolved s i l i c a t e species.
In this way a S i mass balance over the solution and the s o l i d phase during the s i l i c a l i t e synthesis was obtained. The r e s u l t s are summarized i n Table I, which also gives the r e s u l t s of a s i m i l a r procedure for an analogous synthesis i n the presence of DMSO. In t h i s l a t t e r case, however, we were not able to f i l t e r the solution as thoroughly as i n the f i r s t one, so that at the beginning of the synthesis a minor trace of amorphous material was present.