By Prof. Dr. Klaus Weissermel, Prof. Dr. Hans?Jurgen Arpe(auth.)
This bestselling average, now in its fourth, thoroughly revised English version, is a wonderful resource of technological and monetary info at the most vital precursors and intermediates utilized in the chemical undefined. the interpretation into 8 languages and the 5 German and 4 English variations essentially proof the recognition of this book.
'... it's the place i glance first to get a brief review of the producing strategy of a product... Weissermel/Arpe has been serving me for years as an vital reference work.' (Berichte der Bunsengesellschaft fur Physikalische Chemie)
'It will be unkind and deceptive to name this publication a bad man's Kirk Othmer, however it may virtually be defined as an encyclopedia... you'll learn and one has to respect the authors' commitment and undertaking in getting quite a bit right into a unmarried quantity. they've got supplied a booklet that's attention-grabbing analyzing in addition to being an outstanding reference. it's a hugely instructed ebook, which i am hoping the authors will locate the power to proceed updating on a typical basis.' (Chemistry in Britain)
'...it will be able to hand to each chemist or technique engineer concerned without delay or in some way with business natural chemistry. it's going to be within the hand of each higher-graduate pupil, specially if chemical expertise isn't a part of the research, like in lots of collage universities...' (Tenside-Surfactants-Detergents)
Content:
Chapter 1 numerous facets of the power and uncooked fabric provide (pages 1–13):
Chapter 2 easy items of business Syntheses (pages 15–57):
Chapter three Olefins (pages 59–89):
Chapter four Acetylene (pages 91–105):
Chapter five 1,3?Diolefins (pages 107–126):
Chapter 6 Syntheses concerning Carbon Monoxide (pages 127–144):
Chapter 7 Oxidation items Ethylene (pages 145–192):
Chapter eight Alcohols (pages 193–215):
Chapter nine Vinyl?Halogen and Vinyl?Oxygen Compounds (pages 217–238):
Chapter 10 elements for Polyamides (pages 239–266):
Chapter eleven Propene Conversion items (pages 267–312):
Chapter 12 Aromatics — creation and Conversion (pages 313–336):
Chapter thirteen Benzene Derivatives (pages 337–385):
Chapter 14 Oxidation items of Xylene and Naphthalene (pages 388–405):
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Extra resources for Industrial Organic Chemistry, Fourth Edition
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A. a. CH3OH manufacture: from highly compressed synthesis gas (CO/Hz) with many variations of process conditions and catalyst composition modified oxide system based on ZnO-Cr2O3 as first-generation, Cu0-ZnO/Alz03 as second-generation catalysts Methanol is one of the most important industrial synthetic raw materials. Worldwide, about 90% is used in the chemical industry and the remaining 10% is used for energy. 1 x lo6 tonnes, respectively. Japan ceased to produce methanol in 1997 and now imports its entire requirements.
In 1972, the prototype of a large scale plant (310000 tonnes per year) went on stream in Billingham, United Kingdom. Modem plants have an annual production capacity of about one million tonnes. The Cu-Zn-Al-oxide-based catalyst requires a synthesis gas particularly free of sulfur and chlorine. A new generation of catalysts with a 50% longer lifespan was recently introduced. 3. ICI low pressure process (50-100 bar, 240-260°C) process characteristics: Cu-Zn-Al-oxide catalyst requires S- and C1-free synthesis gas and then supplies very pure CHsOH The usual process conditions in the converter are 50-100 bar and 240-260°C.
Allothermal or autothermal heat supply 3. gasification agent 5. process conditions The Winkler gasification, Koppers-Totzek gasification, and the Lurgi pressure gasification are established industrial processes. conventional industrial gasification processes: Winkler Koppers-Totzek Lurgi more recent pilot plant tested gasification processes: Rheinbraun (H2) Bergbau-Forschung (steam) Kellogg (molten NazC03) In addition, second-generation gasification processes such as the Rheinbraun hydrogenative gasification and the BergbauForschung steam gasification in Germany, the Kellogg coal gasification (molten Na2C03) and the Exxon alkali carbonate catalyzed coal gasification in the USA, and the Sumitomo (recently in cooperation with Klockner-Humboldt-Deutz) coal gasification (molten iron) in Japan have reached a state of development where pilot and demonstration plants have been in operation for several years.