Industrial Crystallization by Gregory D. Botsaris (auth.), J. W. Mullin (eds.)

By Gregory D. Botsaris (auth.), J. W. Mullin (eds.)

Industrial Crystallization Symposia were prepared by means of the Crystallization learn staff on the Czechoslovak study Institute for Inorganic Chemistry, Usti nad Labem, considering the fact that 1960. through the years, the expanding acclaim for the unit operation of crystallization has been in actual fact proven via the regular bring up in numbers of either the papers offered and the attendances on the conferences. The sixth Symposium (1-3 September 1975) used to be geared up together with the eu Federation of Chemical Engineering operating get together on Crystallization, and the forty four papers provided have been prepared into 4 periods - A: Secondary Nucleation, B: Crystal progress Kinetics, C: Crystal behavior amendment, D: Crystallizer layout, E: Indus­ trial Crystallizer Operation and Case reviews. a similar groupings are preserved during this edited model of the complaints. this is often the 1st time that the economic Crystallization Symposium papers have seemed in a single quantity. After the fifth (1972) Symposium, authors we.re inspired to put up their papers to a world magazine focusing on crystallization. in spite of the fact that, the implications weren't altogether passable in that below one 3rd of the papers awarded on the assembly have been provided for attention. This time, accordingly, the organizing committee made up our minds to aim to maintain the papers jointly via making preparations for his or her book through Plenum Press.

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21 should be equal to F6 in eq. 11, ~C~ is decided from the intersection point on the plots of F~U and Fb against ~C1' as in the cylindrical crystallizer. DISCUSSION Test data for an industrial cone crystallizer depigned to produce potash alum are shown. 4. The relations between product crystal size, crystallization rate and operational conditions are estimated from laboratory tests by the proposed equations as follows: 1. 81, S2, Z for the given crystallizer, are known 2. ¢ are set 3. E are assumed 4.

Experiments with a Type-2 Crystalliser The results for an industrial crystalliser operating at l20 0 C (first effect) and receiving a clear liquid are summarised in Table 3. Neither milled salt nor small salt cubes were added. The tip velocity of the screw pump was varied. while the circulation rate in m3 /h was kept constant. Conclusion As a result of the work described above crystallisers able to produce salt with an average crystal size (50% by weight) in the range of 200 - 750 jJm can now be built.

F. Strickland-Constable, J. Crystal Growth, 22, 188 (1974). B. Head, J. Crystal Growth, ~, 349 (1970). L. McCabe, AIChE Symposium Series, 68 (121), 31 (1972). W. T. F. Sarofim, AIChE J •• 20, 855 (1974). O~ Soviet Physics-Crystallography, I, 456 (1956). A. F. Str~ckland-Constable, J. Crystal Growth, ~, 1 (1969). R. Wolff, AIChE J. 14, 488 (1968). D. , 19, 510 (1973). P. Moffitt, J. , 19, 433 (1964). , Ind. Eng. Chem. Fundamentals 1, 313 (1964). , J. Chem. Soc. 89, 413 (1906). , MS thesis, Dept.

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