By Abner Brenner
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Extra info for Electrodeposition of Alloys. Principles and Practice
Example text
The relative proportion of the two metals has no effect on the establishment of the equihbrium. The resulting solution then contains a low concentration of the more noble metal, copper, and a relatively high concentration of the less noble metal, bismuth. The ratio by weight of copper to bismuth is 3:97. The equilibrium could also have been accomplished electrochemically by placing a copper electrode in a solution of copper perchlorate and a bismuth electrode in a solu tion of bismuth perchlorate, connecting the solutions by a salt bridge and then shorting the cell.
Wiley, N e w York, 1939. [10] J . GuBKiN, Electrolytische Metallabschneidung an der. freien Oberfläche einer Salzlösung. Ann. Physik [3] 3 2 , 114-115 (1887). [11] A . KLEMENC, N e w way in the application of electrical energy to chemical processes. Chimia 6, 177-180 (1952). [12] A . KLEMENC and W . K O H L , Glimmlichtelektrolyse. X X V . Ü b e r d e n Verlauf der Oxydationsreaktionen bei der Glimmlichtelektrolyse. Monatsh. 8 4 , 498-511 (1953). [13] M . HAISSINSKY and A . COCHE, Reductions anodiques par electrolyse par étincelle.
The data are shown as curve 1 in Fig. 3-1. The maximum in the curve between 57 and 66% of copper does not have any obvious interpreta tion, since this range of composition does not correspond to a phase of brass. Pure beta brass, which contains 45-55% copper, is the phase that lies closest to this range of composition. Curve 2 represents the static potentials obtained by Sauerwald [26] with brass electrodeposited from a sulfate solution. The potentials were measured with the brass immersed in a solution of zinc sulfate.